The Gas Absorption/Desorption Column Apparatus OperatiX - 12 studies mass transfer between gas and liquid phases using a CO2/air mixture and water solvent. This Gas Absorption/Desorption Column Apparatus features a glass, Raschig-ring-packed absorption column paired with a vacuum-operated desorption column for solvent regeneration. It includes continuous pressure, temperature, and flow rate monitoring with liquid and gas sampling outlets. Optional accessories include a water chiller and DAQ software for data measurement and calculation.

Gas Absorption/Desorption Column Apparatus OperatiX - 12, Technical Specifications
| Specification | Detail |
|---|---|
| Process | Absorption in counterflow with water for the separation of the CO2/air combination |
| Gas Mixture Production | Utilizing CO2 from compressed gas cylinders and outside air |
| Mixing Ratio | Valve-based adjustment |
| Gas Delivery | Compressor delivers gas mixture into the absorption column |
| Column Packing | Raschig rings packed inside a glass absorption column |
| Solvent Regeneration | Continuous, in vacuum-sealed circuit with desorption column |
| Absorption Column Pump | Separate pump |
| Hot Water Temperature | Heater-controlled |
| Cold Water Temperature | Chiller control (optional) |
Technical Data
Absorption Column
| Parameter | Value |
|---|---|
| Internal diameter | 100mm approx. |
| Height | 2x 750mm |
| Material | Glass |
Packing
| Parameter | Value |
|---|---|
| Type | Raschig ring |
| Material | Glass |
| Diameter | 10mm |
| Height | 10mm |
Feed Pump (absorption)
| Parameter | Value |
|---|---|
| Max. flow rate | 10L/min |
| Max. head | 10m |
Feed Tank
| Parameter | Value |
|---|---|
| Capacity | 50L |
| Heater | 500W |
For Air and CO2
| Parameter | Value |
|---|---|
| Type | Plate type |
| Material | Stainless steel |
Pressure Sensor
| Parameter | Value |
|---|---|
| Type | Differential |
| Range | -50~50kPa |
| Qty | 2 |
Measuring Ranges
| Parameter | Value |
|---|---|
| Air flow rate | Approx. 0.25~2.5m³/h |
| Solvent flow rate | 1~7lpm |
| CO2 flow rate | 0.1~1m³/h |
| Temperature | 3x -100~400°C |
| Pressure | 1x 0~2.5bar |
| Differential pressure | 2x -25~25kPa |
| CO2 concentration sensor | 0~99% |
Key Features
Experiments
Construction and Design
The Gas Absorption/Desorption Column Apparatus OperatiX - 12 is built around a glass absorption column, 100mm internal diameter, in two 750mm sections. The column is packed with glass Raschig rings, 10mm in diameter and 10mm in height. A compressor delivers the gas mixture into the lower part of the absorption column. A separate feed pump supplies solvent at a maximum flow rate of 10L/min and a maximum head of 10m. A 50L feed tank with a 500W heater supplies water to the system. Plate type, stainless steel units handle air and CO2. Two differential pressure sensors, ranged -50 to 50kPa, monitor pressure loss across the column sections. A desorption column, operating under vacuum, separates absorbed CO2 from the charged water for solvent regeneration. Outlets are provided for collecting liquid and gas samples.
Software
Software OperatiX - 12 (optional). DAQ software specially designed in National Instrument™, LABVIEW™ environment to measure and calculate the results of the apparatus. The software is optional; a set of electronic sensors is included when the software is used. The software can be run in any Windows™ environment.
Scope of Delivery
Optional Accessories
Q: What is the Gas Absorption/Desorption Column Apparatus OperatiX - 12 used for?
A: It is used to study mass transfer from a gaseous phase to a liquid phase (absorption) and the reverse process (desorption), using a CO2/air gas mixture and water as the solvent.
Q: What packing material is used in the absorption column?
A: The absorption column is packed with glass Raschig rings, 10mm in diameter and 10mm in height.
Q: How is the CO2 separated from the solvent?
A: The charged water is supplied to a desorption column, where a vacuum pump creates negative pressure, causing the CO2 gas to escape from the water. The regenerated solvent is then pumped back into the absorption column.
Q: Is a water chiller available for this system?
A: Yes, a Water Chiller, model OperatiX-12-1, is available as a recommended optional accessory for cold water temperature control.
Q: Is data acquisition software available with this system?
A: Yes, Software OperatiX - 12 is available as an optional add-on, designed in National Instrument™ LABVIEW™ environment, and can run in any Windows™ environment.