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Chemical Engineering Lab Equipment List — B.Tech Setup Guide for Process and Chemical Engineering Colleges

The Chemical Engineering laboratory is the practical cornerstone of B.Tech Chemical Engineering and B.Tech Process Engineering programmes. From distillation and extraction to heat transfer and reaction kinetics, the laboratory equipment must cover both unit operations and process control. This guide provides a complete equipment list, specifications, and AICTE norms for chemical engineering laboratory setup.

Chemical Engineering Lab Categories

  • Chemical Process Principles Lab (Semester 3–4)
  • Heat Transfer Operations Lab (Semester 5–6)
  • Mass Transfer Operations Lab (Semester 5–6)
  • Reaction Engineering Lab (Semester 6–7)
  • Process Control and Instrumentation Lab (Semester 5–7)
  • Fluid Mechanics and Hydraulics Lab (Semester 3–4)

Fluid Mechanics and Hydraulics Lab

Equipment Specification
Pipe friction apparatus Laminar/turbulent flow in pipes, manometer bank, 0.01–10 m/s velocity range
Flow measurement apparatus Venturimeter, orifice plate, rotameter in series — hydraulic bench fed
Centrifugal pump test rig H-Q curve, efficiency, NPSH determination; 0.5 kW motor, 50 L/min max flow
Bernoulli’s theorem apparatus Convergent-divergent channel with 8 pressure tappings
Reynolds apparatus Dye injection visualisation of laminar, transitional, turbulent flow regimes
Hydraulic bench Self-contained recirculating water supply, volumetric measurement tank

Heat Transfer Operations Lab

Equipment Specification
Double pipe heat exchanger Co-current and counter-current flow, Cu inner tube 16mm OD, 2m length
Shell and tube heat exchanger 4-pass, 19 tubes × 1.2m, LMTD and overall HTC determination
Plate heat exchanger Stainless steel plates, 0.04 m² area per plate, 20 plates
Forced convection over a tube Blower unit, heated cylinder, thermocouple bank
Condensation and boiling heat transfer Film condensation on a vertical surface, nucleate and film boiling observation
Thermal conductivity apparatus Guarded hot plate method, k determination for insulation materials

Mass Transfer Operations Lab

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Equipment Specification
Distillation column (glass) Bubble cap or sieve plate, 50mm dia, 6-plate column, reflux condenser
Liquid-liquid extraction unit Mixer-settler, 3 stages, glass construction
Packed column (absorption) 50mm dia, Raschig ring packing, CO₂ absorption in NaOH
Tray dryer 4-tray, 60°C to 80°C, airflow measurement
Spray dryer (laboratory scale) Inlet air temp 0–250°C, feed rate 0.1–0.5 L/h, 1.5 kW
Fluidised bed dryer 100mm dia column, variable airflow, pressure drop measurement
Crystallisation unit Batch type, 5 L capacity, cooling crystallisation of salt/sugar solutions
Evaporator (single effect) Climbing film, 0.1 m² heating area, steam or electric heated

Reaction Engineering Lab

Equipment Specification
Continuous stirred tank reactor (CSTR) 2 L glass vessel, variable speed stirrer, pH and temperature monitoring
Plug flow reactor (PFR) Tubular reactor, saponification of ethyl acetate, conductivity monitoring
Batch reactor 5 L glass jacketed, temperature-controlled (0–100°C), stirrer, condenser
Residence time distribution (RTD) apparatus Conductivity-based tracer study for CSTR and PFR

Process Control and Instrumentation Lab

Equipment Specification
Process control trainer (temperature) PID controller, thermocouple, heater, process vessel
Flow control loop Control valve, flow transmitter, PID controller, PC interface
Level control loop Differential pressure transmitter, pneumatic control valve, PC SCADA
Pressure control loop Pressure transmitter, I/P converter, back pressure regulator
Analytical control — pH pH electrode, pH transmitter, acid-base dosing pumps, control valve
Data acquisition system 16-channel, 4–20 mA input, RS-485/USB, SCADA compatible

Safety Equipment (Mandatory for Chemical Labs)

  • Emergency eyewash station — at every lab entrance, ANSI Z358.1 compliant
  • Safety shower — within 10 seconds travel from any chemical workstation
  • Chemical fume hood — minimum 1 per 6 students (100 FPM face velocity)
  • Fire extinguishers — CO₂ for electrical, dry chemical for chemical fires
  • Chemical spill kit — absorbent, neutralising agent, disposal bags
  • Personal protective equipment — goggles, lab coat, chemical-resistant gloves, face shield
  • Ventilation — minimum 10 air changes per hour in all chemical laboratory spaces

Budget Estimate for Chemical Engineering Labs

Lab Approximate Cost (INR)
Fluid Mechanics Lab ₹12–18 lakhs
Heat Transfer Lab ₹15–22 lakhs
Mass Transfer Lab ₹25–40 lakhs
Reaction Engineering Lab ₹15–25 lakhs
Process Control Lab ₹20–35 lakhs
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